Tag Archives: aw-meter

Activ W510 Aw-meter

  • Fanless chilled mirror technology
  • Robust, fast, accurate
  • Very easy cleaning, limited fouling
  • User-friendly interface
  • Automated traceability with Linko PC sofware
  • Low operating costs

Activ W510 specifications
Technology used Chilled mirror, single-stage thermoelectric module
Measurement range Aw 0.030 à 1.000 (HRE: 0.5 à 100%)
Accuracy Aw* +/- 0.003 (HRE: +/- 0.3%)
Repeatability Aw* Standard mode : ± 0.001 (HRE: +/- 0.1%)
Precision mode : ± 0.0005 (HRE: +/- 0.05%)
Room temperature range 0°C à 50°C
Auto detect Water or solvent condensation
Sensor soiling detection
Non-volatile memory 5000 measurements
1024 product datasheets
200 users, 10 users parameters banks
Number of measurement modes Variable time : 3 (Fast, Standard, Precise)
Fixed time : 6 (Flash, 2 min … 1 hour)
Isotherms mode : 2 (consecutive temperature plateaus)
Series of measures One shot to 250 successive measurements
Measurement time Fast mode : 2 to 5 min, depending on your product
Standard mode : 3 to 10 min, depending on your product
Calibration Automatic with 14 different types of saturated / insatured salt solution or manually
A return to factory settings is possible
Dimensions W 24 cm , L 36 cm , H 18 cm
Weight 7.3 Kg without external power supply
Power consumption Active thermoregulation : < 75W/h
Inactive thermoregulation : < 15W/h
Standby : approximately 5W/h
Power requierement External, input 100-240Vac, output 12Vdc 6,25A
Consumables provided Set of 30 plastic dishes with lids
100 ml bottle of saturated salt solution
Warranty 3 years parts and labour

*control salts or homogeneous products, maintenance carried out according to recommendations

Activ W810D Aw-meter

  • Fanless chilled mirror technology
  • Two-stage thermoelectric module
  • Built-in temperature control
  • Robust, fast, accurate
  • Very easy cleaning, limited fouling
  • User-friendly interface
  • Automated traceability with Linko PC sofware
  • Low operating costs

Activ W810D specifications
Technology used Chilled mirror, two-stage thermoelectric module
Measurement range Aw 0.005 à 1.000 (HRE: 0.5 à 100%)
Accuracy Aw* +/- 0.003 (HRE: +/- 0.3%)
Repeatability Aw* Standard mode : ± 0.001 (HRE: +/- 0.1%)
Precision mode : ± 0.0005 (HRE: +/- 0.05%)
Temperature control range Ta – 10°C ≤ setpoint temperature ≤ Ta + 20°C
Ta = ambient temperature
Thermoregulation accuracy 0,1°C
Room temperature range 0°C à 50°C
Auto detect Water or solvent condensation
Sensor soiling detection
Non-volatile memory 5000 measurements
1024 product datasheets
200 users, 10 users parameters banks
Number of measurement modes Variable time : 3 (Fast, Standard, Precise)
Fixed time : 6 (Flash, 2 min … 1 hour)
Isotherms mode : 2 (consecutive temperature plateaus)
Series of measures One shot to 250 successive measurements
Measurement time Fast mode : 2 to 5 min, depending on your product
Standard mode : 3 to 10 min, depending on your product
Calibration Automatic with 14 different types of saturated / insatured salt solution or manually
A return to factory settings is possible
Dimensions W 24 cm , L 36 cm , H 18 cm
Weight 7.3 Kg without external power supply
Power consumption Active thermoregulation : < 75W/h
Inactive thermoregulation : < 15W/h
Standby : approximately 5W/h
Power requierement External, input 100-240Vac, output 12Vdc 6,25A
Consumables provided Set of 30 plastic dishes with lids
100 ml bottle of saturated salt solution
Warranty 3 years parts and labour

*control salts or homogeneous products, maintenance carried out according to recommendations

Syntilab Aw-meters – models


Syntilab measuring instruments are designed, developed and manufactured in France. The new Activ W510 and Activ W810 Water Activity Meters feature modern and innovative technology and are suitable for both laboratory and industrial environments.

  • Fanless chilled mirror technology
  • Single or double stage thermoelectric module
  • Built-in temperature control for the Activ W810
  • Optional connectors for external circulation cryothermostat for Activ W510
  • Robust, fast, accurate
  • Easy cleaning, limited fouling
  • User-friendly interface
  • Automated traceability with “Linko” PC software provided
  • Low operating costs
OUR MODELS OF INSTRUMENTS
Activ W810D Activ W810 Activ W510R Activ W510

MAIN ADVANTAGES

The Activ W510 and Activ W810 models are laboratory meters that perfectly meet the quality and speed standards sought by professionals. Ideally suited for R&D and quality control environments, they are also designed to meet the needs of intensive industrial use on the production line. They are robust and require little maintenance. The technology is based on the chilled mirror principle, which is more precise, faster, more linear and more durable than other technologies.

FANLESS CHILLED MIRROR

The technology used here is patented by Syntilab. It allows fast and accurate measurements without the need for an internal ventilation system. Going fanless is a real technological advance that significantly simplifies the maintenance of a chilled mirror Aw-meter. Its implementation is based on two core elements:

  • a specific geometry and the optimization of the measuring chamber with a minimized internal volume.
  • efficient modeling of heat transfer.

The thermoelectric module for cooling the mirror can be single or double stage depending on the model. The double stage configuration allows measuring highly dehydrated products

MEASUREMENT CHAMBER

One of the main advantages of fanless technology is the limited fouling as well as a higher long-term reliability, as the measuring chamber does not include any moving parts. Its cleaning is facilitated by a direct access to the various elements without disassembly. The micro-measuring chamber as well as the cup receptacle/ dish holder are made entirely of 316L stainless steel which ensures optimum mechanical and chemical resistance, as well as recognized food compatibility. An infrared thermometer measures the temperature of the sample without contact.

THERMAL REGULATION

The Activ W810 features complete and autonomous temperature control of the sample and of the sensor with heat transfer fluid. The setpoint temperature can be set by the user in a range of -10 ° C to + 20 ° C around the ambient temperature.

Requirements for the measurement of water activity according to ISO21807
“… It is recommended to measure Aw at 25 ° C. Variations of ± 1 ° C in the actual measurement temperature have no noticeable effect on water activity … “

The Activ W510 model has no built-in temperature control but can optionally accommodate connectors for the connection of an external circulation thermostatic bath (not supplied).

The instruments can be placed directly in a cold room or in a harsh environment in a range of temperatures from 0 to 50 ° C. The 2017 instrument range benefits from a new sensor with improved thermal insulation. The quality of measurements is not affected in anyway by the proximity of an air conditioner or an oven.

USER INTERFACE

With large color LCD screens, smooth and user-friendly graphic interfaces, and high-capacity internal memories, Syntilab instruments allow optimum measurement use and traceability.

They can be connected to a computer or printer via standard USB and RS232 connectors.

While the instruments are factory-calibrated and offer excellent stability and linearity, they can be very easily controlled and recalibrated with suitable salt solutions. Recalibrations performed by the user can be cancelled if necessary.

These devices feature several modes of configurable measurement, allowing measurement times as fast as 45 seconds, as well as long analyses lasting up to ten days. They can either display Aw or ERH with a selectable 3 or 4 digit resolution. Syntilab Aw-meters are suitable for all types of situations and products, products containing large proportions of volatile substances such as alcohol or propylene glycol must be tested beforehand.

They also have an editable internal database that can store up to 1024 product sheets including the names of the products used, batch numbers and various information such as Aw limit values; water, salt or sugar contents; pH or viscosity. The contents of these sheets can be attached with the measurements made when exporting results to a computer ( see supplied software page ) or a printer.

How to measure water activity ?

The devices measuring water activity are called Aw-meters or Water Activity Meters, they generally comprise a dish holder where a sample cup containing the product to be analyzed can be inserted.

  • Should the samples be crushed ?

The product to be analyzed can be placed in the cup as it is, but it is often crushed/ground or mixed to make it more homogeneous, which considerably speeds up the measurement time of the sample and allows better measurement accuracy.

There is, however, a controversy as to whether or not to crush samples before measuring water activity. The ISO21807 standard does not recommend grinding because of the potential reheating and water loss grinding may cause. Nevertheless, many industries grind their samples before measurement, as it allows quickly homogenizing a product that is not, such as a freshly made product or one that has just been cooked or dried. This homogeneity allows rapid and repeatable measurements representative of the water activity of a product manufactured and stored for some time. We believe that grinding can be useful as long as certain precautions are duly taken, for example:

    • keep a substantial ratio between the ground sample volume and the grinder’s volume, indeed with a limited volume of air in the grinder, water exchange between the sample and the air remains minimal.
    • only use a moderate grinding so as not to modify the matrix of the product and not to overheat it excessively.
  • put a lid on the cup if the sample can not be measured immediately.

In general, the sampling of a product to be measured requires a certain level of cautiousness. The measurement of a large product such as a ham during drying can produce very different results depending on the sampling area. It is therefore necessary to put together a sample consisting of one or more samples – in the same way as coring is used in geology –in order for this sample to be representative of the product as a whole before proceeding with its grinding.

  • Main technologies

Capacitive sensor: A hygroscopic polymer is used as a dielectric. This polymer absorbs or rejects a certain amount of water in relation to the water activity of the measured sample. The resulting variation in electric capacitance makes it possible to deduce the water activity of the sample.

The main advantages of this technology are its rather low cost and a greater insensitivity to volatile substances such as alcohol and propylene glycol.

The main disadvantages of this technology are the loss of efficiency of the sensor over time and fouling issues. The sensor must be recalibrated and/or replaced periodically. Accuracy is lower and it may present some hysteresis. This technology requires several calibration points for the linearity of measurements to be ensured.

Resistive sensor: This technology is very similar to the previous one, only capacitance measurement is replaced by the measurement of the electrical resistance of a sensor made of hygroscopic salt.
This technology also shows a high degree of similarity with the previous one as regards its advantages and disadvantages.

Dew point by mirror cooled: A mirror, coupled with a thermoelectric module and a temperature probe, is chilled until dew appears in its center. The appearance of dew is detected by means of a photodetector. Controlling the amount of dew to a constant value allows to determine the dew point temperature and to then deduce the water activity of the sample.
The main advantages of this technology include very good accuracy, long lifespan and fast measuring time. It is based on a fundamental principle of hygrometric measurement, its natural linearity does not require several calibration points.
The main disadvantage of this technology resides in its greater sensitivity to volatile substances such as alcohol and propylene glycol, that can generate measurement errors. The chilled mirror must be clean for accuracy to be respected.

 Tunable laser diode sensor:This technology called TDLAS for Tunable Diode Laser Absorption Spectroscopy, is of the absorption spectrometry type where the spectrum is extremely narrow and centered on a wavelength specific to the detection of gas phase water. It is a recent technology offering the main advantage of being the most insensitive to volatile substances. Another positive point, that it shares with the chilled mirror, is that there is no hysteresis phenomenon. Accuracy however is lower than that of the chilled mirror ; it requires several calibration points for the linearity of measurements to be effective. It comes at a higher prices and its reliability in time remains to be proven, as this technology has only been available for a few years.

  • Measurement time

Irrespective of the technology used, the measurement of a product’s Aw is done indirectly. It is actually the air contained in the measuring chamber that is analyzed, that is why the measuring chamber must have the smallest possible volume of air while allowing a maximum exchange surface. Water exchanges between the sample and the air contained take place as soon as the measuring chamber is closed. Only when this air is in thermodynamic equilibrium with the measured product will the measurement of Aw be reliable. Most Aw-meters automatically detect a satisfactory equilibrium state, and stop the measurement as necessary.

The measurement time can vary significantly from one product to another. A fat product can form a lipid barrier that will slow down the migration of water, and thus take much longer to measure than another product. Modern devices offer measurement times of often less than 5 minutes, and yet the possibility of performing long-term analyzes represents a significant advantage in that it allows − beyond the simple Aw measurement − understanding the various water migration phenomena that closely depend on it.

  • General Information

Aw-meters often include a non-contact infrared thermometer to measure the temperature of the placed sample.
Water activity devices can be controlled and calibrated using saturated or unsaturated salt solutions, the various existing solutions cover the entire measurement range.
Some devices offer temperature control to make measurements at a stabilized temperature chosen by the user, for example 25 °C which is the temperature recommended by AFNOR, other devices merely measure at room temperature.